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adeola oyelade, s.sasi, F XAvier Castane Sitjas and 3 more joined CHROMmunity 4 hours ago
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Joey Wu and Mohammed Moniruzzaman are now friends Wednesday
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Organic content of sample

Hello everyone,Can someone explain the importance of the organic content of my injected sample. To be more clear; what happens if the organic content of my injected sample is 50% and I run a reverse phase gradient starting at only 10% organic? Is there some kind of rule about this? Something like no more organic difference than 10% between sample and eluent?Any help on this will be truly appreciated. Thanks, BertrandSee More
Discussion posted by BD van Zelst Wednesday
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New with collision cells

Hey guys, not sure if this is a very interesting question, as I am new to MS.  But I was wondering whether or not, there is any advantage in using an hexapole instead of an octapole as a collision cell? Thanks Roberto (your friend from Santa Fe)See More
Discussion posted by Roberto Rodriguez Wednesday
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Mohammed Moniruzzaman left a comment for Dr, T, Michael Harvey
Dear Sir, I am so happy to know that you are from Penang. I am a PhD student of USM health campus, Kelantan. You would be happy to know that my field of research is also analytical chemistry dealing with HPLC, AAS and GC-MS. I would be happy enough…
Wednesday
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GC analysis by headspace

Hello allI am currently trying to analyse Butyl acetate using headspace analysis. I am trying to get  calibration curve but I have been having  some reproducibility issues. For a supposed same concentration I am getting peak areas ranging from 100 to 2000 !.The procedure I am using to prepare my samples is the following:- Seal 155 ml serum bottles with teflon septa crimp top caps  .- Introduce a known amount (10 ul) of B.Ac (liquid) through the septa using a microsyringe- Let it evaporate…See More
Discussion posted by Eduardo Poleo Tuesday
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Quechers

How to ensure proper partitioning of acetonitrile and water in quechers prep in extraction phase?See More
Discussion posted by Bindiya Sameem Jan 19
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March 11, 2012 to March 15, 2012
Join CHROMacademy at the PITTCON Conference & Expo 2012.  Meet Tony Tayor, Technical Director, and other authors of the site for live sign ups.  1 year FREE subscriptions for all University students and staff made available by Agilent Technologies as well as FREE coporate demo accounts for CHROMacademy.See More
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Forum

Roberto Rodriguez

New with collision cells 1 Reply

Started by Roberto Rodriguez in HPLC Posts. Last reply by Jorge Omar Gil Posada on Friday.

BD van Zelst

Organic content of sample 2 Replies

Started by BD van Zelst in HPLC Posts. Last reply by Wang-Yu Kim on Friday.

Eduardo Poleo

GC analysis by headspace 1 Reply

Started by Eduardo Poleo in GC Posts. Last reply by Roberto Rodriguez on Wednesday.

Bindiya Sameem

Quechers 2 Replies

Started by Bindiya Sameem in Sample Prep Posts. Last reply by John M. Dolan Jan 23.

Tamara Strelitzer

Changing RT's in isocratic conditions on Fused Core HPLC columns 6 Replies

Started by Tamara Strelitzer in HPLC Posts. Last reply by Stephanie Schuster Jan 16.

dasarath

perchloric acid is used in HPLC mobile phase 4 Replies

Started by dasarath in HPLC Posts. Last reply by dasarath Jan 16.

Dirk Siekmeier

Colistin in (drinking) Water API MSMS 2 Replies

Started by Dirk Siekmeier in LC-MS & GC-MS Posts. Last reply by Dirk Siekmeier Dec 28, 2011.

Tony Pinho

adding 0,0 corrdinates to linear regression analysis to represent the blank response 16 Replies

Started by Tony Pinho in HPLC Posts. Last reply by Marcelo Coppari Dec 14, 2011.

saptarshi moitra

DIFFERENT AREA OF SAME SAMPLE OF SAME CONCENTRATRATION IN DIFFERENT METHOD 4 Replies

Started by saptarshi moitra in HPLC Posts. Last reply by dasarath Dec 14, 2011.

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Isidre Casals

Amino acid analysis: Moore & Stein versus LC-MS.

Posted by Isidre Casals on December 1, 2011 at 7:32am

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Editorial survey and a chance to win an Apple ipad2

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Dynamic Liquid Sampling to a GC in the past ...

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High-definition GC–MS

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Use ChromWorks SMB model for Control Study

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Paying Attention to POPs

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What do you know about volatile extraction?

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Is chromatography boring?

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Characterising Columns – Have your Say!!

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UHPLC or HPLC? The Choice is Yours

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PREGA v6.1

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Janet Kelsey

Perfect detection with GC–MS

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